Application of SPE for selective fractionation of essential oils constituents from plant materials

Joanna Szewczyk, Michał P. Dybowski, Andrzej L. Dawidowicz

Abstract


Solid-phase extraction (SPE) is simple and inexpensive sample preparation procedure which can be applied for the isolation/fractionation of essential oil compounds from wide variety of samples, such as foodstuffs, biological and environmental. Due to the complex nature of the examined matrices and frequently low concentration level of target components, analytical procedures require the use of initial sample preparation stage. The paper shows the possibility of essential oil components fractionation from different plant materials using SPE method. The results presented in this paper shows that the proposed SPE procedure allows for easy and total fractionation of essential oil constituents (especially low-molecular oxygen compounds) from the sample matrix.

Keywords


SPE; essential oils from herbs; fractionation

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References


A. Antonelli, C. Fabbri, Chromatographia, 49, 125-130, (1999).

A.L. Dawidowicz, E. Rado, D. Wianowska, J. Sep. Sci., 32, 3034-3042, (2009).

M. Gilar, E.S.P. Bouvier, B.J. Compton, J. Chromatogr. A, 909, 111-135, (2001).

T. Fornari, G. Vicente, E. Vázquez, M.R. García-Risco, G. Reglero, J. Chromatogr. A, 1250, 34– 48, (2012).

Y. Picó, M.J. Ruiz, G. Font, J. Biochem. Biophys. Meth., 70, 117-31, (2007).

Ph. Morin, M. Caude, H. Richard, R. Rosset, J. Chromatogr. A, 363, 57-69, (1986).

E.D. Guerrero, F. Chinnici, N. Natali, R.N. Martin, C. Riponi, J. Sep. Sci., 31, 3030–3036, (2008).

T. Fornari, G. Vicente, E. Vázquez, M.R. García-Risco, G. Reglero, J. Chromatogr. A, 1250, 34-48, (2012).

S.M. Pourmortazavi, S.S. Hajimirsadeghi, J. Chromatogr. A, 1163, 2–24, (2007).

S.R. Yousefi, F. Shemirani, Microchim Acta, 173, 415–421, (2011).

N. Sahraoui, M.A. Vianb, I. Bornard, Ch. Boutekedjiret, F. Chema, J. Chromatogr. A, 1210, 229–233, (2008).

M. Jalali Heravi, H. Sereshti, J. Chromatogr. A, 1160, 81–89, (2007).

G. Özek, F. Demirci, T. Özek, N. Tabanca, D.E. Wedge, S.I. Khan, K.H. Baser, A. Durand, E. Hamzaoglu, J. Chromatogr. A, 1217, 741–748, (2010).

R.M. Smith, J. Chromatogr. A, 1000, 3–27, (2003).

T. Fornari, G. Vicente, E. Vázquez, M.R. García-Risco, G. Reglero, J. Chromatogr. A, 1250, 34–48, (2012).

A.L. Dawidowicz, D. Wianowska, E. Rado, Phytochem. Anal., 22, 51-58, (2011).

R. Castro, R. Natera, E. Durán, C. García-Barroso, Eur. Food. Res. Technol., 228, 1–18, (2008).

A. Żwir-Ferenc, M. Biziuk, Polish J. of Environ., 15, 677-690, (2006).

Z. Cobb, L.I. Andersson, Anal. Bioanal. Chem., 383, 645–650, (2005).

M.S. Beldean-Galea, C. Horga, M.V. Coman, Cent. Eur. J. Chem., 8, 1110–1116, (2010).

C.I. Rodrigues, L. Marta, R. Maiaa, M. Mirandab, M. Ribeirinhob, C. Maguas, J. Food Compos. Anal., 20, 440–448, (2007).

C.W. Huie, Anal. Bioanal. Chem., 373, 230-30, (2002).

Z. Piñeiro, M. Palma, C.G. Barroso, Anal. Chim. Acta, 513, 209–214, (2004).

Laurence Berthod, G. Roberts, G.A. Mills, J. Pharm. Anal., 4, 117-124, (2014).




DOI: http://dx.doi.org/10.17951/aa.2015.70.2.87
Date of publication: 2016-02-15 12:20:03
Date of submission: 2016-02-15 11:03:01


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Copyright (c) 2016 Joanna Szewczyk, Michał P. Dybowski, Andrzej L. Dawidowicz