Synthesis and characterization of mesoporous silica: laboratory exercises for students

Marek Kosmulski, Edward Mączka

Abstract


Synthesis and characterization of SBA-15 were proposed as a laboratory course: linked series of exercises for graduate students. The standard preparation method was modified to fit a typical schedule of students’ classes, that is, 3-hours units every second week. The properties of materials obtained by different students’ groups were compared with the properties of materials obtained by means of a standard method.


Keywords


SBA-15; specific surface area; zeta potential;

Full Text:

PDF

References


D.Y. Zhao, J.L. Feng, Q.S. Huo, N. Melosh, G.H. Fredrickson, B.F. Chmelka, and G.D. Stucky, Science, 279, 548, (1998).

M. Barczak, E. Skwarek, W. Janusz, A. Dąbrowski, and S. Pikus, Appl.Surf.Sci., 256, 5370, (2010).

A.W. Marczewski, A. Deryło-Marczewska, I. Skrzypek, S. Pikus, and M.Kozak, Adsorption, 15, 300, (2009).

A. Deryło-Marczewska, A.W. Marczewski, I. Skrzypek, S. Pikus, and M. Kozak, Appl.Surf.Sci., 255, 2851, (2008).

M. Kokunesoski, J. Gulicovski, B. Matovic, M. Logar, S.K. Milonjic, and B. Babic, Mater.Chem.Phys., 124, 1248, (2010).

J.M. Rosenholm, M. Linden, Chem. Mater. 19, 5023, (2007).

H. Perez, P. Navarro, M. Montes, Chem. Eng. J. 158, 325, (2010).

A. Nieto, F. Balas, M. Colilla, M. Manzano, M-Vallet-Regi, Microp.Mesop. Materials, 116, 4 (2008).

T.X. Bui, H.C. Choi, J. Hazard. Mat. 168, 602, (2009).




DOI: http://dx.doi.org/10.17951/aa.2016.71.2.59
Data publikacji: 2017-04-03 12:28:05
Data złożenia artykułu: 2016-10-14 11:49:55

Refbacks

  • There are currently no refbacks.


Copyright (c) 2017 Marek Kosmulski, Edward Mączka